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Number of results: 47
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Abstract

Equal-channel angular pressing (ECAP) was used as a technique for severe plastic deformation (SPD) on Al alloy AA3004. This technique produced fully dense materials of refined grain structure to sub-micrometer dimensions and advanced mechanical properties. The ECAP processing of samples was conducted as 1 to 4 passes through the die at room temperature. We present the results of the studied homogeneity evolution with the ECAP treatment. Furthermore, a Scanning Electron Microscope (SEM) was used for examination of the microstructure changes in samples undergone from 1 to 4 passes. The microhardness-HV increased upon each ECAP pass. The resulting micro-hardness evolution was attributed to crystalline microstructure modifications, such as the d-spacing (studied by X-ray Diffraction-XRD) depending on the number of ECAP pressings. The microcrystalline changes (grain refining evaluated from the Scanning Electron Microscopy – SEM images) were found to be related to the HV, following the Hall-Petch equation.
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Abstract

In the dissertation the data modeling has been shown for the data that regards the damages, which value is above zero. With the use of Weibull distribution, with prior regression and correlation analysis chosen parameters that defines the life time and failure level of two populations of AlSi17Cu5 were defined. The calculation sheet of reliability allows to create so called survival diagram, and on the basis of durability data the average warrantee can be determined, on the pre-exploitation period.
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Abstract

This paper presents the results of hypoeutectic 226 grade alloy as well as prepared on its basis Al-Si alloy containing Cr, V and Mo. The additives tested were added as AlCr15, AlV10 and AlMo8 master alloys. Alloys tested were poured into DTA sampler as well as using pressure die casting. An amount of Cr, V and Mo additives in alloy poured into DTA sampler comprised within the range approximately 0.05-0.35%. Alloys to pressure die casting contained 0.05-0.20% Cr, V and Mo. The crystallization process was examined using the derivative thermal analysis (DTA). The microstructure of castings made in the DTA sampler as well as castings made with use of pressure die casting were examined. The basic mechanical properties of castings made using pressure die casting were defined too. It has been shown in the DTA curves of Al-Si alloy containing approximately 0.30 and 0.35% Cr, Mo, and V there is an additional thermal effect probably caused by a peritectic crystallization of intermetallic phases containing the aforementioned additives. These phases have a morphology similar to the walled and a relatively large size. The analogous phases also occur in pressure die casting alloys containing 0.10% or more additions of Cr, V and Mo. The appearance of these phases in pressure die casting Al-Si alloys coincides with a decrease in the value of the tensile strength Rm and the elongation A. It has been shown die castings made of Al-Si alloys containing the aforementioned additives have a higher Rm and A than 226 alloy.
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Abstract

In the dissertation it has been shown, that so called „time-thermal treatment” (TTT) of the alloy in liquid state, as overheating the metal with around 250o C above the Tliq. and detaining it in this temperature for around 30 minutes, improves the mechanical properties (HB, Rm, R0,2). It was ascertained, that overheating the AlSi17Cu5Mg alloy aids the modification, resulting with microcrystalline structure. Uniform arrangement of the Si primeval crystals in the warp, and α(Al) solution type, supersaturated with alloying elements present in the base content (Cu, Mg) assures not only increased durability in the ambient temperature, but also at elevated temperature (250o C), what is an advantage, especially due to the use in car industry.
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Abstract

Iron is the most common and detrimental impurity in casting alloys and has been associated with many defects. The main consequence of the presence or adding of iron to AlSi alloys is the formation Fe-rich intermetallics with especially deleterious β-Al5FeSi. β-Al5FeSi phases are most often called needles on 2D micro sections, whilst platelets in 3D geometry. The x-ray tomography results have demonstrated Ferich phases with shapes different from simple forms such as needles or platelets and presented bent and branched phases. β grown as complicated structure of bent and branched intermetallics can decrease feeding ability, strengthen pores nucleation and eutectic colonies nucleation leading to lower permeability of mushy zone and porosity in the castings.
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Abstract

This paper deals with influence on segregation of iron based phases on the secondary alloy AlSi7Mg0.3 microstructure by nickel. Iron is the most common and harmful impurity in aluminum casting alloys and has long been associated with an increase of casting defects. In generally, iron is associated with the formation of Fe-rich intermetallic phases. It is impossible to remove iron from melt by standard operations. Some elements eliminates iron by changing iron intermetallic phase morphology, decreasing its extent and by improving alloy properties. Realization of experiments and results of analysis show new view on solubility of iron based phases during melt preparation with higher iron content and influence of nickel as iron corrector of iron based phases.
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Abstract

Currently there is a constant development in the field of aluminium alloys engineering. This results from, i.a., better understanding of the mechanisms that direct strengthening of these alloys and the role of microalloying. Now it is microalloying in aluminum alloys that is receiving a lot of attention. It affects substantially the macro- and microstructure and kinetics of phase transformation influencing the properties during production and its exploitation. 7xxx series aluminum alloys, based on the Al-Zn-Mg-Cu system, are high-strength alloys, moreover, the presence of Zr and Sr further increases their strength and improves resistance to cracking. This study aims to present the changes of the properties, depending on the alloy chemical composition and the macro- and microstructure. Therefore, the characteristics in the field of hardness, tensile strength, yield strength and elongation are shown on selected examples. Observations were made on ingot samples obtained by semi-continuous casting, in the homogenized state. Samples were prepared from aluminum alloys in accordance with PN-EN 573-3: 2013. The advantage of Al-Zn-Mg-Cu alloys are undoubtedly good strength, Light-weight and resistance to corrosion. As widening of the already published studies it is sought to demonstrate the repeatability of the physical parameters in the whole volume of the sample.
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Abstract

With the use of differential scanning calorimetry (DSC), the characteristic temperatures and enthalpy of phase transformations were defined for commercial AlSi9Cu3 cast alloy (EN AC-46000) that is being used for example for pressurized castings for automotive industry. During the heating with the speed of 10oCmin-1 two endothermic effects has been observed. The first appears at the temperature between 495 oC and 534 oC, and the other between 555 oC and 631 oC. With these reactions the phase transformation enthalpy comes up as +6 J g-1 and +327 J g-1 . During the cooling with the same speed, three endothermic reactions were observed at the temperatures between 584 oC and 471 oC. The total enthalpy of the transitions is – 348 J g-1 . Complimentary to the calorimetric research, the structural tests (SEM and EDX) were conducted on light microscope Reichert and on scanning microscope Hitachi S-4200. As it comes out of that, there are dendrites in the structure of α(Al) solution, as well as the eutectic (β) silicon crystals, and two types of eutectic mixture: double eutectic α(Al)+β(Si) and compound eutectic α+Al2Cu+β.
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Abstract

The paper presents the results of studies on the effect of the AlSi17Cu5 alloy overheating to atemperature of 920°C and modification with phosphorus (CuP10) on the resultingmechanical (HB, Rm, R0.2) and plastic (A5 and Z) properties. It has been shown that, so-called, "timethermal treatment" (TTT) of an alloy in the liquid state, consisting inoverheating the metal to about 250°C above Tliq,holding at this temperature by 30 minutes improvesthe mechanical properties. It has also been found that overheating of alloy above Tliq.enhances the process of modification, resulting in the formation of fine-grain structure. The primary silicon crystals uniformly distributed in the eutectic and characteristics ofthe α(Al) solution supersaturated with alloying elements present in the starting alloy composition (Cu, Fe) provide not only an increase of strength at ambient temperature but also at elevated temperature (250°C).
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Abstract

The article presents the investigations of 7xxx aluminium alloys performed by the method of thermal and derivational analysis. The studies made it possible to identify the effect of the changes in the Cu concentration, the total Zn and Mg weight concentrations and the Zn/Mg weight concentration ratio on their crystallization process: the cooling as well as the kinetics and dynamics of the thermal process of cooling and crystallization. Metallographic studies were performed on the microstructure of the examined alloys and their HB hardness was measured. The evaluation of the changes was presented in reference to the model alloys EN AW-7003 and EN AW-7010, whose microstructure under the conditions of thermodynamic equilibrium are described by the phase diagrams: Al-Zn-Mg and Al-Zn-Mg-Cu. The performed investigations confirmed that the hardness HB of the examined alloys is mainly determined by the reinforcement of the matrix αAl by the introduced alloy additions and the presence of phases Θ(Al2Cu) and S(Al2CuMg) rich in copper, as well as η(MgZn2), in the examined alloys' microstructure. The increase of the amount of intermetallic phases precipitated in the microstructure of the examined alloys is caused, beside Cu, by the characteristic change of Zn wt. concentration and Mg. It was proposed that the process of one-stage thermal treatment of the examined alloys be introduced at a temperature of up to tJ-20 °C, which will prevent the exceedance of the solidus temperature.
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Abstract

Directional solidification technique is an important research instrument to study solidification of metals and alloys. In the paper the model [6,7,8] of directional solidification in special Artemis-3 facility was presented. The current work aimed to propose the ease and efficient way in calibrating the facility. The introduced M coefficient allowed effective calibration and implementation of defined thermal conditions. The specimens of AlSi alloys with Fe-rich intermetallics and especially deleterious β-Al5FeSi were processed by controlled solidification velocity, temperature gradient and cooling rate.
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Abstract

Solidification of AlSiFe alloys was studied using a directional solidification facility and the CALPHAD technique was applied to calculate phase diagrams and to predict occurring phases. The specimens solidified by electromagnetic stirring showed segregation across, and the measured chemical compositions were transferred into phase diagrams. The ternary phase diagrams presented different solidification paths caused by segregation in each selected specimen. The property diagrams showed modification in the sequence and precipitation temperature of the phases. It is proposed in the study to use thermodynamic calculations with Thermo-Calc which enables us to visualize the mushy zone in directional solidification. 2D maps based on property diagrams show a mushy zone with a liquid channel in the AlSi7Fe1.0 specimen center, where significant mass fraction (33%) of β-Al5FeSi phases may precipitate before α-Al dendrites form. Otherwise liquid channel occurred almost empty of β in AlSi7Fe0.5 specimen and completely without β in AlSi9Fe0.2. The property diagrams revealed also possible formation of α–Al8Fe2Si phases.
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Abstract

The paper presents the results of the application of a statistical analysis to evaluate the effect of the chemical composition of the die casting Al-Si alloys on its basic mechanical properties. The examinations were performed on the hypoeutectic Al-Si alloy type EN AC-46000 and, created on its basis, a multi-component Al-Si alloy containing high-melting additions Cr, Mo, W and V. The additions were introduced into the base Al-Si alloy in different combinations and amounts (from 0,05% to 0,50%). The tensile strength Rm; the proof stress Rp0,2; the unit elongation A and the hardness HB of the examined Al-Si alloys were determined. The data analysis and the selection of Al-Si alloy samples without the Cr, Mo, W and V additions were presented; a database containing the independent variables (Al-Si alloy's chemical composition) and dependent variables (Rm; Rp0,2; A and HB) for all the considered variants of Al-Si alloy composition was constructed. Additionally, an analysis was made of the effect of the Al-Si alloy's component elements on the obtained mechanical properties, with a special consideration of the high-melting additions Cr, Mo, V and W. For the optimization of the content of these additions in the Al-Si alloy, the dependent variables were standardized and treated jointly. The statistical tools were mainly the multivariate backward stepwise regression and linear correlation analysis and the analysis of variance ANOVA. The statistical analysis showed that the most advantageous effect on the jointly treated mechanical properties is obtained with the amount of the Cr, Mo, V and W additions of 0,05 to 0,10%.
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Abstract

The study presents the results of the application of a statistical analysis for the evaluation of the effect of high-melting additions introduced into a pressure cast Al-Si alloy on the obtained level of its proof stress Rp0.2. The base Al-Si alloy used for the tests was a typical alloy used for pressure casting grade EN AC-46000. The base alloy was enriched with high-melting additions, such as: Cr, Mo, V and W. The additions were introduced into the base Al-Si alloy in all the possible combinations. The content of the particular high-melting addition in the Al-Si alloy was within the scope of 0.05 to 0.50%. The investigations were performed on both the base alloy and alloy with the high-melting element additions. Within the implementation of the studies, the values of Rp0.2 were determined for all the considered chemical compositions of the Al-Si alloy. A database was created for the statistical analysis, containing the independent variables (chemical composition data) and dependent variables (examined Rp0.2 values). The performed statistical analysis aimed at determining whether the examined high-melting additions had a significant effect on the level of Rp0.2 of the Al-Si alloy as well as optimizing their contents in order to obtain the highest values of the Al-Si alloy's proof stress Rp0.2. The analyses showed that each considered high-melting addition introduced into the Al-Si alloy in a proper amount can cause an increase of the proof stress Rp0.2 of the alloy, and the optimal content of each examined high-melting addition in respect of the highest obtained value of Rp0.2 equals 0.05%.
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Abstract

The research focused on the influence of the solution temperature on the structure of precipitation hardening multi-component hypoeutectic aluminium alloys. The AlSi8Cu3 and AlSi6Cu4 alloys were used in the study and were subjected to a thermal-derivative analysis. The chemical composition and crystallization of phases and eutectics shift the characteristic points and the corresponding temperatures to other values, which affect to, for instance, the solution temperature. The alloys were supersaturated at 475°C (according to the determined temperature (TSol) and 505°C for 1.5 hours. Aging was performed at 180°C for 5 hours. The Rockwell hardness measurement, metallographic analysis of alloys by means of light microscopy as well as chemical and phase analysis using scanning electron microscopy and X-ray crystallography were carried out on alloys. The use of computer image analysis enabled the determination of the amount of the current Al2Cu phase in the alloys before and after heat treatment.
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Abstract

The paper presents tribological properties of A390.0 (AlSi17Cu5Mg) alloy coupled in abrasive action with EN-GJL-350 grey cast-iron. The silumin was prepared with the use of two different technologies which differed in terms of cooling speed. In the first case the alloy was modified with foundry alloy CuP10 and cast to a standard tester ATD and in case of second option the modified alloy was cast into steel casting die. Due to different speed of heat removal the silumins varied in structure, particularly with size of primary crystals of silicon and their distribution in matrix which had a significant influence of friction coefficient in conditions of dry friction.
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Abstract

The microscale deformation behaviour of the Al-4.5Cu-2Mg alloy has been studied to understand the influence of various processing routes and conditions, i.e. the gravity casting with and without grain refiner, the rheocast process and the strain induced melt activation (SIMA) process. The micromechanics based simulations have been carried out on the optical microstructures of the alloy by 2D representative volume elements (RVEs) employing two different boundary conditions. Microstructural morphology, such as the grain size, the shape and the volume fraction of α-Al and binary eutectic phases have a significant effect on the stress and strain distribution and the plastic strain localization of the alloy. It is found that the stress and strain distribution became more uniform with increasing the globularity of the α-Al grain and the α-Al phase volume fraction. The simulated RVEs also reveals that the eutectic phase carries more load, but least ductility with respect to the α-Al phase. The SIMA processed alloy contains more uniform stress distribution with less stress localization which ensures better mechanical property than the gravity cast, grain refined and rheocast alloy.
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Abstract

The aim of the paper is the residual stress analysis of AlSi10Mg material fabricated by selective laser melting (SLM). The SLM technique allows to product of complex geometries based on three-dimensional model, in which stiffness and porosity can be precisely designed for specific uses. As the studied material, there were chosen solid samples built in two different directions: parallel (P-L) and perpendicular (P-R) to the tested surface and cellular lattice built in perpendicular direction, as well. In the paper, for the complex characterization of obtained materials, the phase analysis, residual stress and texture studies were performed. The classical non-destructive sin2ψ method was used to measure the residual stress measurements. The final products, both solid sample and cellular lattice, have a homogeneous phase composition and consist of solid solution Al(Si) (Fm-3m) type, Si (Fd-3m) and Mg2Si (Pnma). The obtained values of the crystallite size are in a range of 1000 Å for Al(Si), 130-180 Å for Si phase. For Mg2Si phase, the crystallite sizes depend on sintering process, they are 800 Å for solid samples and 107 Å for cellular lattice. The residual stress results have the compressive character and they are in a range from –5 to –15 MPa.
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Abstract

The paper concerns the problem of discontinuity in high pressure die castings (HPDC). The compactness of their structure is not perfect, as it is sometimes believed. The discontinuities present in these castings are the porosity as follow: shrinkage and gas (hydrogen and gas-air occlusions) origin. The mixed gas and shrinkage nature of porosity makes it difficult to identify and indicate the dominant source. The selected parameters of metallurgical quality of AlSi9Cu3 alloy before and after refining and the gravity castings samples (as DI - density index method), were tested and evaluated. This alloy was served to cast the test casting by HPDC method. The penetrating testing (PT) and metallographic study of both kinds of castings were realized. The application of the NF&S simulation system allowed virtually to indicate the porosity zones at risk of a particular type in gravity and high-pressure-die-castings. The comparing of these results with the experiment allowed to conclude about NF&S models validation. The validity of hypotheses concerning the mechanisms of formation and development of porosity in HPDC casting were also analyzed.
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Abstract

Railway buffers during the operation are staying in almost permanent contact with each other, creating friction node in the point of contact of two railway buffer heads. In consequence of overcoming track curves, turnouts and unevenness of track, the railway buffer heads moves relative to each other causing friction, which results in its wear. When the wear is excessive, it might be a reason to withdrawn vehicle from service, it causes flattening of buffer head, and in consequence its abnormal cooperation. To avoid this phenomenon the buffer heads should be covered with graphitized grease, but this method has many disadvantages. Accordingly, it was found that it would be beneficial to cover the buffer head with bronze using laser cladding. In this article the metallographic and mechanical analysis of the newly created top layer of railway buffer head are presented. In article the results from tribological tests conducted on Amsler test bench are also presented. Based on test results described in article concluded that the layer of bronze coat on working surface of railway buffer head can be beneficial from operational point of view.
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Abstract

The impact of casting conditions on microstructure a and mechanical properties was described, especially for cast products from AlSi9Cu3 alloy. Particular attention was paid to the parameters of dendritic structure: DAS 1 and DAS 2. Selected mechanical properties (by static tension test) of test castings made using basic technologies of casting: GSC - gravity sand casting, GDC - gravity die-casting and HPDC - high-pressure die-casting, are presented for cast-on test bars and cast separately. Casts were made of the same alloy AlSi9Cu3. Fractures and the zone near the fracture (after static tension test) was subjected to VT - visual tests, PT - penetration tests and metallographic tests. The condition of porosity (fracture zone) was also assessed. The analysis of virtual results was performed using the NovaFlow & Solid system together with the database and they were compared to experimental tests. This way of validation was applied in order to assess the correlation between the local rate of cooling and the size of DAS for GSC, GDC and HPDC technologies. Finally, the correlation between the parameters of structure and mechanical properties with regard to the impact of porosity was signalized.
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