The high-pressure torsion (HPT) of Ti-Fe alloys with different iron content has been studied at 7 GPa, 5 anvil rotations and rotation speed of 1 rpm. The alloys have been annealed before HPT in such a way that they contained different amounts of α/α' and β phases. In turn, the β phase contained different concentration of iron. The 5 anvil rotations correspond to the HPT steady-state and to the dynamic equilibrium between formation and annihilation of microstructure defects. HPT leads to the transformation of initial α/α' and β-phases into mixture of α and high-pressure ω-phase. The α → ω and β → ω phase transformations are martensitic, and certain orientation relationships exist between α and ω as well as β and ω phases. However, the composition of ω-phase is the same in all samples after HPT and does not depend on the composition of β-phase (which is different in different initial samples). Therefore, the martensitic (diffusionless) transformations are combined with a certain HPT-driven mass-transfer. We observed also that the structure and properties of phases (namely, α-Ti and ω-Ti) in the Ti – 2.2 wt. % Fe and Ti – 4 wt. % Fe alloys after HPT are equifinal and do not depend on the structure and properties of initial α'-Ti and β-Ti before HPT.
Recent research in the process of aluminum alloy die castings production, which is nowadays deeply implemented into the rapidly growing automobile, shipping and aircraft industries, is aimed at increasing the useful qualitative properties of the die casting in order to obtain its high mechanical properties at acceptable economic cost. Problem of technological factors of high pressure die casting has been a subject of worldwide research (EU, US, Japan, etc.). The final performance properties of die castings are subjected to a large number of technological factors. The main technological factors of high pressure die casting are as follows: plunger pressing speed, specific (increase) pressure, mold temperature as well as alloy temperature. The contribution discusses the impact of the plunger pressing speed and specific (increase) pressure on the mechanical properties of the casting aluminum alloy.
Experimental Mg-Al-RE type magnesium alloys for high-pressure die-casting are presented. Alloys based on the commercial AM50 magnesium alloy with 1, 3 and 5 mass % of rare earth elements were fabricated in a foundry and cast in cold chamber die-casting machines. The obtained experimental casts have good quality surfaces and microstructure consisting of an α(Mg)-phase, Al11RE3, Al10RE2Mn7 intermetallic compound and small amount of α+γ eutectic and Al2RE phases.
The paper describes issues related to pressure drop that accompanies the phenomenon of maldistribution of working fluid between the channels of a model minichannel plate heat exchanger. The research concerns a single exchanger’s plate containing 51 (in every geometry) parallel rectangular minichannels of hydraulic diameters 461 μm, 571 μm, 750 μm, and 823 μm. In addition, more complex geometry has been investigated, equipped with additional diagonal channels (so called extended geometry). The moment of the liquid phase transition through the heat exchanger was recorded at the flow rates ranging from 0.83 g/s to 13.33 g/s in the inlet manifold. The paper discusses the total pressure drop as a function of the flow rate and the characteristic dimension of minichannels, as well as the pressure drop as a function of the time of the fluid passage through the main part of the measuring section in which measurements were done. The resulting profiles correlate with the images of the flow distribution between channels recorded using the fast shutter speed camera, that allows to draw a further conclusions about the specifics of the maldistribution process. The impact of the total pressure drop on the actual range of optimum operating conditions of the heat exchanger was analyzed.
The work presents the results of the investigations of the effect of the nitrogen (N2) refining time „τraf” and the gas output on the course of the crystallization process, the microstructure and the gassing degree of silumin 226 used for pressure casting. The refinement of the examined silumin was performed with the use of a device with a rotating head. The crystallization process was examined by way of thermal analysis and derivative analysis TDA. The performed examinations showed that the prolongation of the N2 refining time causes a significant rise of the temperature of the crystallization end of the silumin, „tL”, as well as a decrease of its gassing degree, „Z”. An increase of the nitrogen output initially causes an increase of the temperature „tL” and a drop of the gassing degree „Z”, which reach their maximal values with the output of 20 dm3 /min. Further increase of the output causes a decrease of the value „tL” and an increase of „Z”. The examined technological factors of the refining process did not cause any significant changes in the microstructure of silumin 226.
The work presents the effect of strontium and antimony modification on the microstructure and mechanical properties of 226 silumin casts. The performed research demonstrated that strontium causes high refinement of silicon precipitations in the eutectic present in the microstructure of the examined silumin and it significantly affects the morphology of eutectic silicon from the lamellar to the fibrous one. Sr modification also causes an increase of: the tensile strength „Rm” by 12%; the proof stress „Rp0,2” by 5%; the unit elongation „A” by 36% and the hardness HB by 13%. Antimony did not cause a change in the microstructure of the silumin, yet it caused an increase in Rm and HB by 5%, in Rp0,2 by 7% and in A by 4%.
The results of statistical analysis applied in order to evaluate the effect of the high melting point elements to pressure die cast silumin on its tensile strength Rm, unit elongation A and HB were discussed. The base alloy was silumin with the chemical composition similar to ENAC 46000. To this silumin, high melting point elements such as Cr, Mo, V and W were added. All possible combinations of the additives were used. The content of individual high melting point additives ranged from 0.05 to 0.50%. The tests were carried out on silumin with and without above mentioned elements. The values of Rm, A and HB were determined for all the examined chemical compositions of the silumin. The conducted statistical analysis showed that each of the examined high melting point additives added to the silumin in an appropriate amount could raise the values of Rm, A and HB. To obtain the high tensile strength of Rm = 291 MPa in the tested silumin, the best content of each of the additives should be in the range of 0.05-0.10%. To obtain the highest possible elongation A of about 6.0%, the best content of the additives should be as follows: chromium in the range of 0.05-0.15%, molybdenum 0.05% or 0.15%, vanadium 0.05% and tungsten 0.15%. To obtain the silumin with hardness of 117 HB, chromium, molybdenum and vanadium content should be equal to about 0.05%, and tungsten to about 0.5%.
This paper presents the effect of the temperature and hold time in the holding furnace of 226 silumin on the characteristic quantities of TDA curves. The temperature of phase transformations and the cooling rate were tested.It has been shown that increasing both the hold time and the temperature in the holdingfurnace cause the decreasethe end ofα+Al9Fe3Si2+β and α+Al2Cu+βternary eutectics crystallizationtemperature in the tested silumin. This is due to the fact an increase in amounts of impurities as a result of reacting theliquid alloy with the gases contained in the air.It has been shown, however, that examined technological factors ofthe metal preparation do not cause systematic changes in the cooling rate.
The research described in this contribution is focused on fractographic analysis of the fracture area of newly developed eutectic silumin type AlSi9NiCuMg0.5 (AA 4032), which was developed and patented by a team of staff of the Faculty of Mechanical Engineering. The paper presents determination of the cause of casting cracks in operating conditions. Fractographic analysis of the fracture area, identification of the structure of the casting, identification of structural components on the surface of the fracture surface and chemical analysis of the material in the area of refraction were performed within the experiment. Al-Si alloys with high specific strength, low density, and good castability are widely used in pressure-molded components for the automotive and aerospace industries. The results shown that the inter-media phases Fe-Al and Fe-Si in aluminium alloys lead to breakage across the entire casting section and a crack that crossed the entire cross section, which was confirmed by EDS analysis.
Materials and their development process are highly dependent on proper experimental testing under wide range of loading within which high-strain rate conditions play a very significant role. For such dynamic loading Split Hopkinson Pressure Bar (SHPB) is widely used for investigating the dynamic behavior of various materials. The presented paper is focused on the SHPB impulse measurement process using experimental and numerical methods. One of the main problems occurring during tests are oscillations recorded by the strain gauges which adversely affect results. Thus, it is desired to obtain the peak shape in the incident bar of SHPB as “smooth” as possible without any distortions. Such impulse characteristics can be achieved using several shaping techniques, e.g. by placing a special shaper between two bars, which in fact was performed by the authors experimentally and subsequently was validated using computational methods.
Gas atmosphere at the sand mould/cast alloy interface determines the quality of the casting obtained. Therefore the aim of this study was to measure and evaluate the gas forming tendency of selected moulding sands with alkyd resins. During direct and indirect gas measurements, the kinetics of gas evolution was recorded as a function of the temperature of the sand mixture undergoing the process of thermal destruction. The content of hydrogen and oxygen was continuously monitored to establish the type of the atmosphere created by the evolved gases (oxidizing/reducing). The existing research methodology [1, 7, 8] has been extended to include pressure-assisted technique of indirect measurement of the gas evolution rate. For this part of the studies, a new concept of the measurement was designed and tested. This article presents the results of measurements and compares gas emissions from two sand mixtures containing alkyd resins known under the trade name SL and SL2002, in which the polymerization process is initiated with isocyanate. Studies of the gas forming tendency were carried out by three methods on three test stands to record the gas evolution kinetics and evaluate the risk of gas formation in a moulding or core sand. Proprietary methods for indirect evaluation of the gas forming tendency have demonstrated a number of beneficial aspects, mainly due to the ability to record the quantity and composition of the evolved gases in real time and under stable and reproducible measurement conditions. Direct measurement of gas evolution rate from the tested sands during cast iron pouring process enables a comparison of the results with the results obtained by indirect methods.
The pressure drop in microreactors for the gas - liquid Taylor flow was measured for 4 different microreactor geometries and 3 different gas - liquid systems. The results have been compared with the existing literature correlations. A selection of the best correlations has been made.
The aim of the study was to determine species structure of aquatic bugs in four anthro-pogenic water reservoirs. Heteroptera structure observed in studied reservoirs was clearly differen-tiated, which refers to age of the ponds. Newly created water reservoirs become quickly colonized mainly by pioneering species Corixinae, which led to formation of taxonomic group population of density exceeding 2700 indiv. m-2. In older reservoirs there were fish, which potential predation pressure led to almost a complete decline of bugs. The reason of bugs poverty in water reservoirs colonized by fish was also probably a small habitat diversity, leading to lack of refuges from predators.
The upper section of the Bystrzyca River has a character of trout and grayling zone of river. The aim of the study was to determine the species composition of fish in the upper section of the Bystrzyca River and attempt to evaluate angling pressure on fish in this section of river based on analysis of records of amateur fishing. To determine the fish composition the control fishing was conducted using electric fishing gear. The assessment of angling pressure was based on the analysis of 2135 records of fishing in the mountain type rivers in 2012 year, obtained from PAA Lublin. The brown trout and grayling were a dominant fish species in the upper section of the Bystrzyca River, and the first of them was present on the whole length of the river and had the highest average density. The changes of fish community along the river course from Salmonids lead to an increase of the share of Cyprinids fish has been observed. Analysis of records of ama-teur fish catch revealed that the upper section of the Bystrzyca River is under considerable of angling pressure and the most commonly fished species was brown trout. However, the properly carried fishery management on this section of river and the establishment of „no kill” zone allows for proper maintenance of the populations of fish species valuable for anglers.
The paper presents a method for wireless measurement of car wheel air pressure and temperature using the Tire Pressure Monitoring System, or TPMS module - one of the latest safety systems introduced by the automotive industry - with readings taken on a specifically designed test bench. The paper describes the structure and operating principle of the test bench key elements and how they work with the sensors, the TPMS module, and reference instruments, as well as the data format and accuracy of data transmission between TPMS and the host computer. The software designed for an embedded system emulating the real on-board computer allows for observing raw sensor readings and the effect of calibration in two points of the characteristics.
The subject presented in this paper refers to measurements and assessment of the corrected sound pressure level values (noise) occurring around a medium-power transformer. The paper presents the values of noise accompanying the operation of the power object before and after its modernization, which consisted in repeated core pressing and replacement of the cooling system. The main aim of the research work was the assessment of the influence of the repair work on the noise level emitted into the environment.
The Neumann boundary value problem for the Helmholtz equation within the quarter-space has been considered in this paper. The Green function has been used to find the acoustic pressure amplitude as the approximation valid within the Fraun-hoffer's zone for some time-harmonic steady state processes. The low fluid loading has been assumed and the acoustic attenuation has been neglected. It has also been assumed that the vibration velocity of the acoustic particles is small as compared with the sound velocity in the gaseous medium.
Acoustic radiation sources are successfully applied to cleaning rooms from dust of fairly large particle sizes (ten micrometers and larger). The sedimentation of fine aerosols (particle diameter of 1-10 microns) is a more complicated challenge. The paper is devoted to the substantiation of the acoustic sedimentation method for such aerosols. On the basis of the mathematical model analysis for aerosol sedimentation by the acoustic field the mechanisms of this process have been determined and include the particle coagulation acceleration and radiation pressure effect. The experimental results of the acoustic sedimentation of a model aerosol (NaCl) are shown. The calculation results according to the mathematical model for coagulation and sedimentation, on the basis of the Smolukhovsky’s equation taking into account various mechanisms of aerosol sedimentation by sound depending on the particle sizes and sound intensity, are given. The necessity to use intensive sources of high-frequency sound has been confirmed, suggesting that these sources must be located above dust clouds.
The paper deals with the impact of technological parameters on the mechanical properties and microstructure in AlSi12 alloy using squeeze casting technology. The casting with crystallization under pressure was used, specifically direct squeeze casting method. The goal was to affect crystallization by pressure with a value 100 and 150 MPa. From the experiments we can conclude that operating pressure of 100 MPa is sufficient to influence the structural characteristics of the alloy AlSi12. The change in cooling rate influences the morphology of the silicon particles and intermetallic phases. A change of excluded needles to a rod-shaped geometries with significantly shorter length occurs when used gravity casting method. At a pressure of 100 MPa was increased of tensile strength on average of 20%. At a pressure of 150 MPa was increased of tensile strength on average of 30%. During the experiment it was also observed, that increasing difference between the casting temperature and the mold temperature leads to increase of mechanical properties.
The article concerns investigations over benefits of application of HRC devices into sulphide copper ore processing plant. High pressure comminution appears to be very effective technology in hard ore processing circuits, especially in terms of energy consumption. This can be particularly observed in downstream grinding and beneficiation operations. A series of pilot-scale crushing tests in HRC roller press for various levels of operating pressure, were performed. HRC crushing effectiveness along with downstream grinding process course for each crushing product were also under analysis. The investigations were supplemented by analysis of flotation process effectiveness and impact of the process of high-pressure comminution on environment (dust emission). The results of investigation show that operating pressure level influences the obtained comminution results (comminution degree, yield of finest particle size fractions). The grinding effectiveness, measured through production of the finest particle size fractions was significantly influenced by the operating pressure. The results show that higher values of operating pressure (4.0 and 4.5 N/mm2) are not as efficient within this scope as the pressure 3.5 N/mm2. Dust emission is also correlated with the operating pressure value.
In the paper the analysis of random vibration of an actively damped laminated plate with functionally graded piezoelectric actuator layers is presented. The simply supported plate is subjected to stochastic loading represented by a uniformly distributed pressure. The random input is assumed as a Gaussian sta- tionary and ergodic process. The actuators are regarded as a multi-layer structure arranged of piezofiber composite sub-layers. The sub-layers differ each other with amount of PZT (lead-zirconate-titanate) fibers and are stacked to achieve a desired change of the PZT volume fraction through the actuator thickness. The gradation scheme of constituents and material properties are estimated by parabolic and power functions. Numerical simulations are performed to recognize the influence of the applied random excita- tions and the actuator properties gradations on the characteristics of the stochastic field of active plate deflection i.e. power spectral density, autocorrelation function and variance
This work presents a simulation of the response of packets of microbubbles in an ultrasonic pulse-echo scan line. Rayleigh-Plesset equation has been used to predict the echo from numerically obtained radial dynamics of microbubbles. Varying the number of scattering microbubbles on the pulse wave form has been discussed. To improve microbubble-specific imaging at high frequencies, the subharmonic and second harmonic signals from individual microbubbles as well as microbubbles packets were simulated as a function of size and pressure. Two different modes of harmonic generation have been distinguished. The strength and bandwidth of the subharmonic component in the scattering spectrum of microbubbles is greater than that of the second harmonic. The pressure spectra provide quantitative and detailed information on the dynamic behaviour of ultrasound contrast agent microbubbles packet.
In this study, the effect of gas pressure on the shape and size of the AZ91 alloy powder produced by using the gas atomization method was investigated experimentally. Experiments were carried out at 820°C constant temperature in 2-mm nozzle diameter and by applying 4 different gas pressures (0.5, 1.5, 2.5 and 3.5 MPa). Argon gas was used to atomize the melt. Scanning electron microscope (SEM) to determine the shape of produced AZ91 powders, XRD, XRF and SEM-EDX analysis to determine the phases forming in the internal structures of the produced powders and the percentages of these phases and a laser measuring device for powder size analysis were used. Hardness tests were carried out to determine the mechanical properties of the produced powders. The general appearances of AZ91 alloy powders produced had general appearances of ligament, acicular, droplet, flake and spherical shape, but depending on the increase in gas pressure, the shape of the powders is seen to change mostly towards flake and spherical. It is determined that the finest powder was obtained at 820°C with 2 mm nozzle diameter at 3.5 MPa gas pressure and the powders had complex shapes in general.
Magnesium alloys are one of the lightest of all the structural materials. Because of their excellent physical and mechanical properties the alloys have been used more and more often in various branches of industry. They are cast mainly (over 90%) on cold and hot chamber die casting machines. One of the byproducts of casting processes is process scrap which amounts to about 40 to 60% of the total weight of a casting. The process scrap incorporates all the elements of gating systems and fault castings. Proper management of the process scrap is one of the necessities in term of economic and environmental aspects. Most foundries use the process scrap, which involves adding it to a melting furnace, in a haphazard way, without any control of its content in the melt. It can lead to many disadvantageous effects, e.g. the formation of a hard buildup at the bottom of the crucible, which in time makes casting impossible due to the loss of the alloy rheological properties. The research was undertaken to determine the effect of an addition of the process scrap on the mechanical properties of AZ91 and AM50 alloys. It has been ascertained that the addition of a specific amount of process scrap to the melt increases the mechanical properties of the elements cast from AZ91 and AM50 alloys. The increase in the mechanical properties is caused mainly by compounds which can work as nuclei of crystallization and are introduced into the scrap from lubricants and anti-adhesive agents. Furthermore carbon, which was detected in the process scrap by means of SEM examination, is a potent grain modifier in Mg alloys [1-3]. The optimal addition of the process scrap to the melt was determined based on the statistical analysis of the results of studies of the effect of different process scrap additions on the mean grain size and mechanical properties of the cast parts.
The paper presents the results of experimental heat transfer and pressure drop during condensation of the single component refrigerant R134a and zeotropic mixtures R404A, R407C, and R410A in tube minichannels of internal diameter from the range 0.31–3.30 mm. The local values and the average of heat transfer coefficient and pressure drop in the whole range of the change in mass quality were measured. On the basis of the obtained test results there was illustrated the influence of the change of mass vapor quality, the mass flux density, and the inner diameter of channel on the studied parameters. These results were compared with the calculation results based on the relations postulated by other authors. The discrepancy range was ± 50%. On the basis of given test results own correlation was developed to calculate the heat transfer coefficient and pressure drop of tested refrigerants which presents the obtained results in a range of discrepancy of ±25%.