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Abstrakt

In the present work, amine based extractant and its mixture with cationic and solvating extractants were tested for the extraction of HCl from chloride solution containing Al(III). The chloride feed solution resulted from the leaching of spent HDS (hydro-desulfurization) catalysts. For this purpose, amine extractants, such as TOA (trioctyl amine), Alamine 336 (a mixture of tri-octyl/decyl amine), Alamine 308 (tri-isooctyl amine), and TEHA (tri 2-ethylhexyl amine) were used and the extraction and stripping behavior of HCl was compared. The extracted HCl was easily stripped from loaded TEHA phase, when compared with the other tested tertiary amine system. Solvent extraction reaction of HCl by TEHA was determined from the extraction data. Unlike TOA and Alamine 336, adding cationic extractant to TEHA had negligible effect on the extraction and stripping of HCl. In our experimental ranges, no Al was extracted by amines and pure HCl was recovered. MaCabe- Thiele diagrams for the extraction and stripping of HCl by TEHA were constructed.
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The paper presents an analysis of the voicing of the phoneme /v/ in modern spoken Macedonian. The phoneme /v/ in the standard Macedonian language is classifi ed as a fricative, but some of its characteristics separate it from the other phonemes in this group. This is due to the fact that this phoneme was once a sonorant. In a part of the Macedonian dialects this phoneme is pronounced with marked voicing to this day. This phenomenon is then refl ected in the pronunciation of standard Macedonian. Our analysis is based on a selected corpus of examples that have been spoken by speakers from various dialect origins, in order to assess the any differences in pronouncing of the phoneme /v/ when placed in different phoneme contexts in the word.
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A novel phase shift full bridge (PSFB) converter with voltage-doubler and decoupling integrated magnetics in photovoltaic (PV) systems is proposed. Considering the demand that the output voltage is higher than the input voltage in PV systems, the voltage-doubler is added to achieve higher voltage gain compared with the traditional PSFB. In order to avoid current oscillation caused by the voltage-doubler and obtain the wide zero voltage switching (ZVS) ranges, an external inductor is imposed on the circuit. Especially, to obtain much higher power density, the external inductor and transformer are integrated into one magnetic core. The operation and voltage gain of proposed converter are analyzed. Also, in order to reveal the effects the integrated magnetics gives to the converter, the decoupling condition and the expression of leakage inductor of integrated magnetics are obtained in detail. Finally a 100 W prototype converter is made and the experimental results are given to verify the analysis.
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The paper is focused on properties testing of materials used in form of iso-exo sleeves for risers in ferrous alloys foundry. They are grainyfibrous materials, containing components which initiate and upkeep exothermic reaction. Thermo-physical parameters characterizing such sleeves are necessary also to fill in reliable databases for computer simulation of processes in the casting-mould layout. Studies with use of a liquid alloy, especially regarding different sleeves bring valuable results, but are also relatively expensive and require longer test preparation time. A simplified method of study in laboratory conditions was proposed, in a furnace heated to a temperature above ignition temperature of sleeve material (initiation of exothermic reaction). This method allows to determine the basic parameters of each new sleeve supplied to foundries and assures relatively quick evaluation of sleeve quality, by comparison with previous sleeve supplies or with sleeves brought by new providers.
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The paper summarizes research realized by the author in laboratory and industrial conditions (foundries of cast steel and cast iron, castings up to 50 tons) on the effects of the chemically hardened molding sands regeneration using hard/soft rubbing in the dry reclamation. A reference was simultaneously made to advisability of application of the thermal regeneration in conditions, where chromite amount in the circulating (reclaimed) molding sand goes as high as above ten percent. An advisability of connecting standard and specialized methods of examination of the reclaimed sands and molding sands made using it was pointed out. A way of application of studies with the Hot Distortion Plus® method modified by the author for validation of modeling of the thermo-dynamic phenomena in the mold was shown.
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The paper presents an original method of measuring the actual chromite content in the circulating moulding sand of foundry. This type of material is applied for production of moulds. This is the case of foundry which most frequently perform heavy casting in which for the construction of chemical hardening mould is used, both the quartz sand and chromite sand. After the dry reclamation of used moulding sand, both types of sands are mixed in various ratios resulting that in reclaimed sand silos, the layers of varying content of chromite in mixture are observed. For chromite recuperation from the circulating moulding sand there are applied the appropriate installations equipped with separate elements generating locally strong magnetic field. The knowledge of the current ratio of chromite and quartz sand allows to optimize the settings of installation and control of the separation efficiency. The arduous and time-consuming method of determining the content of chromite using bromoform liquid requires operational powers and precautions during using this toxic liquid. It was developed and tested the new, uncomplicated gravimetric laboratory method using powerful permanent magnets (neodymium). The method is used in the production conditions of casting for current inspection of chromite quantity in used sand in reclamation plant.
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The powerful tool for defect analysis is an expert system. It is a computer programme based on the knowledge of experts for solving the quality of castings. We present the expert system developed in the VSB-Technical University of Ostrava called ‘ESWOD’. The ESWOD programme consists of three separate modules: identification, diagnosis / causes and prevention / remedy. The identification of casting defects in the actual form of the system is based on their visual aspect.
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Cell culture transplantation is very promising in the treatment of various diseases. Cells obtained from a number of sources have been analysed to provide a basis for further studies in the area of regenerative medicine. The objective of the study was to compare morphological and phenotypic changes in cat adipose tissue and bone marrow cell cultures from the first to fifth passages. Adipose tissue and bone marrow were used to obtain cell cultures (coming from 3 cats) using standard methods with own modification. Phenotype changes were monitored by CD-marker identification and CD pan-keratin. The cytogenetic analysis was performed on 50 metaphase plates of cell cultures from the first to fifth passage. Cytogenetic assays showed that the adipose tissue cell culture (ATCC) at all passages was more stable than the bone marrow cell culture (BMCC).
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This paper proposes a speech enhancement method using the multi-scales and multi-thresholds of the auditory perception wavelet transform, which is suitable for a low SNR (signal to noise ratio) environment. This method achieves the goal of noise reduction according to the threshold processing of the human ear's auditory masking effect on the auditory perception wavelet transform parameters of a speech signal. At the same time, in order to prevent high frequency loss during the process of noise suppression, we first make a voicing decision based on the speech signals. Afterwards, we process the unvoiced sound segment and the voiced sound segment according to the different thresholds and different judgments. Lastly, we perform objective and subjective tests on the enhanced speech. The results show that, compared to other spectral subtractions, our method keeps the components of unvoiced sound intact, while it suppresses the residual noise and the background noise. Thus, the enhanced speech has better clarity and intelligibility.
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In order to compare the pathogenicity of different Tembusu virus (TMUV) strains from geese, ducks and chickens, 56 5-day-old Cherry Valley ducklings which were divided into 7 groups and infected intramuscularly with 7´105 PFU/ml per duck of six challenge virus stocks. The clinical signs, weight gain, mortality, macroscopic and microscopic lesions, virus loads in sera of 1, 3, 5, 7, 11 and 14 dpi and serum antibody titers were examined. The results showed that these viruses could make the young ducks sick, but the clinical signs differed with the different species-original strains. All the experimental groups lose markedly in weight gain compared to the control, but there were no obvious distinctions in weight gains, as well as macroscopic and microscopic lesions of dead ducks between the infected groups. However, the groups of waterfowl-derived strains (from geese and ducks) showed more serious clinical signs and higher relative expressions of virus loads in sera than those from chicken-derived. The mortality of waterfowl groups was 37.5%, and the greatest mortality of chicken groups was 12.5%. The serum antibodies of the geese-species group JS804 appeared earlier and were higher in the titers than others. Taken toghter, the pathogenicity of waterfowl-derived TMUV was more serious than chicken-derived TMUV and JS804 could be chosen as one TMUV vaccine strain to protect from the infection.
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The main work of this paper focuses on the simulation of binary alloy solidification using the phase field model and adaptive octree grids. Ni-Cu binary alloy is used as an example in this paper to do research on the numerical simulation of isothermal solidification of binary alloy. Firstly, the WBM model, numerical issues and adaptive octree grids have been explained. Secondary, the numerical simulation results of three dimensional morphology of the equiaxed grain and concentration variations are given, taking the efficiency advantage of the adaptive octree grids. The microsegregation of binary alloy has been analysed emphatically. Then, numerical simulation results of the influence of thermo-physical parameters on the growth of the equiaxed grain are also given. At last, a simulation experiment of large scale and long-time has been carried out. It is found that increases of initial temperature and initial concentration will make grain grow along certain directions and adaptive octree grids can effectively be used in simulations of microstructure.
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Objective: This study aimed to investigate developmental changes of the thymus and intra- thymic IL-1β, IL-6 and TNF-α expression in weaned Sprague-Dawley rats induced by lipopolysac- charide. Methods: Forty healthy weaned rats aged 26 days and weighing 83±4 g were randomly and equally divided into two groups. The lipopolysaccharide group was treated daily with a single injection of lipopolysaccharide for 10 consecutive days, and the saline group was treated with an equal volume of sterilized saline. On the 1st, 4th, 7th and 10th day, histological changes and distribu- tion of IL-1β-, IL-6- and TNF-α-positive cells were detected in the thymus by hematoxylin-eosin and immunohistochemistry staining, respectively. Subsequently, the expression levels of IL-1β, IL-6 and TNF-α were evaluated in the thymus by the ELISA method. Results: Thymus weight and index were significantly smaller in lipopolysaccharide-treated rats than in saline-treated rats (p<0.05), but no substantial changes were found in the thymus microstructure after lipopolysaccharide induction. Moreover, a large number of IL-1β-, IL-6- and TNF-α-positive cells were observed with brownish-yellow color and mainly distributed in the thy- mus parenchyma, both integrated optical density and average optical density increased signifi- cantly in lipopolysaccharide-treated rats than those in saline-treated rats. Compared with the saline group, most of the thymic homogenates had higher levels of IL-1β, IL-6 and TNF-α in the lipopolysaccharide group on different days. Conclusion: These findings indicate that the thymus atrophied after lipopolysaccharide induction in weaned Sprague-Dawley rats, and excessive production of intrathymic IL-1β, IL-6 and TNF-α was probably involved in the atrophic process.
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In order to overcome the shortcomings of the dolphin algorithm, which is prone to falling into local optimum and premature convergence, an improved dolphin swarm algorithm, based on the standard dolphin algorithm, was proposed. As a measure of uncertainty, information entropy was used to measure the search stage in the dolphin swarm algorithm. Adaptive step size parameters and dynamic balance factors were introduced to correlate the search step size with the number of iterations and fitness, and to perform adaptive adjustment of the algorithm. Simulation experiments show that, comparing with the basic algorithm and other algorithms, the improved dolphin swarm algorithm is feasible and effective.
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The distortion of air gap magnetic field caused by the rotor eccentricity contributes to the electromechanical coupling vibration of the brushless DC (BLDC) permanent magnet in-wheel motor (PMIWM) in electric vehicles (EV). The comfort of the BLDC in-wheel motor drive (IWMD) EV is seriously affected. To deeply investigate the electromechanical coupling vibration of the PMIWM under air gap eccentricity, the PMIWM, tyre and road excitation are analyzed first. The influence of air gap eccentricity on air gap magnetic density is investigated. The coupling law of the air gap and the unbalanced magnetic force (UMF) is studied. The coupling characteristics of eccentricity rate, air gap magnetic density, UMF, phase current and vibration acceleration are verified on the test bench in the laboratory. The mechanism of the electromechanical coupling vibration of the BLDC PMIWM under air gap static eccentricity (SE), dynamic eccentricity (DE) and hybrid eccentricity (HE) is revealed. DE and HE deteriorate the vibration acceleration amplitude, which contributes the electromechanical coupling vibration of the PMIWM. The research results provide a solid foundation for the vibration and noise suppression of the PMIWM in distributed drive EV.
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In the present work, the performance of multilayer coated carbide tool was investigated considering the effect of cutting parameters during turning of 34CrMo4 Low alloy steel. It has high strength and creep strength, and good impact tenacity at low temperature. It can work at –110°C to 500°C. And EN 10083-1 34CrMo4 owns high static strength, impact tenacity, fatigue resistance, and hardenability; without overheating tendencies. The objective functions were selected in relation to the parameters of the cutting process: surface roughness criteria. The correlations between the cutting parameters and performance measures, like surface roughness, were established by multiple linear regression models. Highly significant parameters were determined by performing an Analysis of variance (ANOVA). During the experiments flank wear, cutting force and surface roughness value were measured throughout the tool life. The results have been compared with dry and wet-cooled turning. Analysis of variance factors of design and their interactions were studied for their significance. Finally, a model using multiple regression analysis between cutting speed, fee rate and depth of cut with the tool life was established.
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At present, with the increase of production capacity and the promotion of production, the reserves of most mining enterprises under the original industrial indexes are rapidly consumed, and the full use of low-grade resources is getting more and more attention. If mining enterprises want to make full use of low-grade resources simultaneously and obtain good economic benefits to strengthening the analysis and management of costs is necessary. For metal underground mines, with the gradual implementation of exploration and mining projects, capital investment and labor consumption are dynamic and increase cumulatively in stages. Consequently, in the evaluation of ore value, we should proceed from a series of processes such as: exploration, mining, processing and the smelting of geological resources, and then study the resources increment in different stages of production and the processing. To achieve a phased assessment of the ore value and fine evaluation of the cost, based on the value chain theory and referring to the modeling method of computer integrated manufacturing open system architecture (CIMOSA), the analysis framework of gold mining enterprise value chain is established based on the value chain theory from the three dimensions of value-added activities, value subjects and value carriers. A value chain model using ore flow as the carrying body is built based on Petri nets. With the CPN Tools emulation tool, the cycle simulation of the model is carry out by the colored Petri nets, which contain a hierarchical structure. Taking a large-scale gold mining enterprise as an example, the value chain model is quantified to simulate the ore value formation, flow, transmission and implementation process. By analyzing the results of the simulation, the ore value at different production stages is evaluated dynamically, and the cost is similarly analyzed in stages, which can improve mining enterprise cost management, promote the application of computer modeling and simulation technology in mine engineering, more accurately evaluate the economic feasibility of ore utilization, and provide the basis for the value evaluation and effective utilization of low-grade ores.
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We studied the thermophilous grass Bromus erectus in Central Europe to determine its pattern of population genetic structure and genetic diversity, using ISSR-PCR fingerprinting to analyze 200 individuals from 37 populations. We found three genetic groups with a clear geographic structure, based on a Bayesian approach. The first group occurred west and south of the Alps, the second east and north of the Alps, and the third was formed by four genetically depauperated populations in Germany. The populations from Germany formed a subset of the Bohemian-Moravian populations, with one private allele. Two differentiation centers, one in the Atlantic- Mediterranean and the second in the Pannonian-Balkan area, were recognized by species distribution modeling. The geographic distribution of the genetic groups coincides with the syntaxonomic split of the Festuco-Brometea class into the Festucetalia valesiaceae and Brometalia erecti orders. We found a statistically significant decrease in mean ISSR bands per individual from south to north, and to a lesser extent from the east to west. The former was explained by Holocene long-distance migrations from southern refugia, the latter by the difference in the gradient of anthropopression. We hypothesize a cryptic northern shelter of the species in Central Europe in the putative Moravian-Bohemian refugium.
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LED light must be cooled to avoid reaching a certain temperature. Two different 3D practical domains of LED light are modelled, (i) square aluminium plate with a cylindrical plate and an LED module (model I), (ii) the same provision of model I with 25 fins (model II). ANSYS 16.0 is used for solving the problem. Temperature distribution, junction temperature (Tj) and heat flux are estimated. Analyses are carried out for various ambient temperatures (Ta) and for different LED power dissipations (Q) to identify the safe operating conditions. In model I, it is found that 38% of working conditions go beyond the critical limit of Tj and it is reduced to 21.4% in model II. In model II, for low Ta of 30 and 40ºC with all Q considered in this analysis are safer. If Ta is between 30 and 80ºC, then Q must be maintained at 0.5 to 1.25 W. Beyond this, conditions are not safe.
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Constantly developing production process and high requirements concerning the quality of glass determine the need for continuous improvement of tools and equipment needed for its production. Such tools like forms, most often made of cast-iron, are characterized by thick wall thickness compared to their overall dimensions and work in difficult conditions such as heating of the surface layer, increase of thermal stresses resulting from the temperature gradient on the wall thickness, occurrence of thermal shock effect, resulting from cyclically changing temperatures during filling and emptying of the mould. There is no best and universal method for assessing how samples subjected to cyclic temperature changes behave. Research on thermal fatigue is a difficult issue, mainly due to the instability of this parameter, which depends on many factors, such as the temperature gradient in which the element works, the type of treatment and the chemical composition of the material. Important parameters for these materials are at high temperature resistance to thermal shock and thermal fatigue what will be presented in this paper.
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The work presents the investigation results concerning the structure of composite pressure die castings with AlSi11 alloy matrix reinforced with SiC particles. Examination has been held for composites containing 10 and 20 volume percent of SiC particles. The arrangement of the reinforcing particles within the matrix has been qualitatively assessed in specimens cut out of the castings. The index of distribution was determined on the basis of particle count in elementary measuring fields. The tensile strength, the yield point and elongation of the obtained composite were measured. Composite castings were produced at various values of the piston velocity in the second stage of injection, diverse intensification pressure values, and various injection gate width values. The regression equation describing the change of the considered arrangement particles index and mechanical properties were found as a function of the pressure die casting parameters. The infuence of particle arrangement in composite matrix on mechanical properties these material was examined and the functions of correlations between values were obtained. The conclusion gives the analysis and the interpretation of the obtained results.
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