This paper presents the results on the effects of die-casting process on the strength parameters of castings of the aluminium AlSi9Cu3 alloy belonging to the group of EN AB-46000, made on renovated high pressure die-casting machine. Specimens for quality testing were taken from the places of the casting most loaded during the service. The aim of a research was to prove how the new die-casting process control capabilities influence on the tensile strength of the cast material defined as a value of the breaking force of the specimens. It has been found that it is possible to specify a set of recommended settings valves of second (II) and third (III) phase, which are responsible for filling the metal mould on die-casting pressure machine. From the point of view of the finished cast element, it was noticed that exceeding the prescribed values of valve settings does not bring further benefits and even causes unnecessary overload and reduce the durability of the mold. Moreover, it was noticed that reduction of the predetermined setting of the second phase (II) valve leads to the formation of casting defects again.
The paper presents the results of hypoeutectic silumin 226 grade and silumin produced on its basis through the addition of V and Mo. Vanadium and molybdenum were added as the preliminary alloy AlV10 and AlMo8 in an amount providing the concentration of 0.1; 0.2; 0.3 and 0.4% V and Mo. TDA curves of tested silumins were presented; regardless of the chemical composition there were similar thermal effects. Pressure castings microstructure research revealed the presence in silumins with the addition of V and Mo phases do not occur in silumin without these additives. These phases have a morphology similar to the walled, and their size increases with increasing concentration of V and Mo. The size of the precipitates of these phases silumin containing 0.1% V and Mo does not exceed 10 microns, while 0.4% of the content of these elements increases to about 80 microns. Tests of basic mechanical properties of silumins were carried out. It has been shown that the highest values of tensile strength Rm = 295 MPa and elongation A = 4.2% have silumin containing approximately 0.1% V and Mo. Increasing concentrations of these elements causes a gradual lowering of the Rm and A values.
The paper presents the results of the computer simulations of solidification with consideration of the liquid phase movement. Simulations were conducted in a real, complex cast. There is a multi-stage resolution to the problem of convection in solidification simulations. The most important resolution concerns the development of the numerical model with the momentum and continuity equations, as well as conditions which are determined by the convection. Simulations were carried out with the use of our authorial software based on stabilized finite elements method (Petroy-Galerkin). In order to solve Navier-Stokes equation (with the convection element), Boussinesq’s approximation were used. Finite Elements Method (FEM) was responsible for the solidification. FEM is close to the heat conduction equation solution (with the internal heat source responsible for the heat released during phase transformation). Convection causes movement in the liquid phase in the solidifying cast and can significantly influence the process of heat transfer from the cast. It may change the distribution of the defects. Results of this article make it possible to assess the conditions in which the influence of the convection on solidification is significant.
This paper presents the results of hypoeutectic 226 grade alloy as well as prepared on its basis Al-Si alloy containing Cr, V and Mo. The additives tested were added as AlCr15, AlV10 and AlMo8 master alloys. Alloys tested were poured into DTA sampler as well as using pressure die casting. An amount of Cr, V and Mo additives in alloy poured into DTA sampler comprised within the range approximately 0.05-0.35%. Alloys to pressure die casting contained 0.05-0.20% Cr, V and Mo. The crystallization process was examined using the derivative thermal analysis (DTA). The microstructure of castings made in the DTA sampler as well as castings made with use of pressure die casting were examined. The basic mechanical properties of castings made using pressure die casting were defined too. It has been shown in the DTA curves of Al-Si alloy containing approximately 0.30 and 0.35% Cr, Mo, and V there is an additional thermal effect probably caused by a peritectic crystallization of intermetallic phases containing the aforementioned additives. These phases have a morphology similar to the walled and a relatively large size. The analogous phases also occur in pressure die casting alloys containing 0.10% or more additions of Cr, V and Mo. The appearance of these phases in pressure die casting Al-Si alloys coincides with a decrease in the value of the tensile strength Rm and the elongation A. It has been shown die castings made of Al-Si alloys containing the aforementioned additives have a higher Rm and A than 226 alloy.
The paper presents the results of the application of a statistical analysis to evaluate the effect of the chemical composition of the die casting Al-Si alloys on its basic mechanical properties. The examinations were performed on the hypoeutectic Al-Si alloy type EN AC-46000 and, created on its basis, a multi-component Al-Si alloy containing high-melting additions Cr, Mo, W and V. The additions were introduced into the base Al-Si alloy in different combinations and amounts (from 0,05% to 0,50%). The tensile strength Rm; the proof stress Rp0,2; the unit elongation A and the hardness HB of the examined Al-Si alloys were determined. The data analysis and the selection of Al-Si alloy samples without the Cr, Mo, W and V additions were presented; a database containing the independent variables (Al-Si alloy's chemical composition) and dependent variables (Rm; Rp0,2; A and HB) for all the considered variants of Al-Si alloy composition was constructed. Additionally, an analysis was made of the effect of the Al-Si alloy's component elements on the obtained mechanical properties, with a special consideration of the high-melting additions Cr, Mo, V and W. For the optimization of the content of these additions in the Al-Si alloy, the dependent variables were standardized and treated jointly. The statistical tools were mainly the multivariate backward stepwise regression and linear correlation analysis and the analysis of variance ANOVA. The statistical analysis showed that the most advantageous effect on the jointly treated mechanical properties is obtained with the amount of the Cr, Mo, V and W additions of 0,05 to 0,10%.
This paper describes the possibility of using very short periods of solution annealing in the heat treatment of unmodified hypoeutectic silumin alloy AlSi7Mg0,3 casted by method of casting with crystallization under pressure with forced convection (direct squeeze casting process). Castings prepared at different casting parameters were subjected to special heat treatment called SST (Silicon Spheroidization Treatment), which were originally used only for the modified silumin alloys to spheroidization of eutectic silicon. Temperature holding time in solution annealing of T6 heat treatment is limited in the SST process to only a few minutes. It was studied the effect of casting parameters and periods of solution annealing on ultimate strength, yield strength, and especially ductility that in the unmodified silumin alloy castings is relatively low.
The study presents the results of the application of a statistical analysis for the evaluation of the effect of high-melting additions introduced into a pressure cast Al-Si alloy on the obtained level of its proof stress Rp0.2. The base Al-Si alloy used for the tests was a typical alloy used for pressure casting grade EN AC-46000. The base alloy was enriched with high-melting additions, such as: Cr, Mo, V and W. The additions were introduced into the base Al-Si alloy in all the possible combinations. The content of the particular high-melting addition in the Al-Si alloy was within the scope of 0.05 to 0.50%. The investigations were performed on both the base alloy and alloy with the high-melting element additions. Within the implementation of the studies, the values of Rp0.2 were determined for all the considered chemical compositions of the Al-Si alloy. A database was created for the statistical analysis, containing the independent variables (chemical composition data) and dependent variables (examined Rp0.2 values). The performed statistical analysis aimed at determining whether the examined high-melting additions had a significant effect on the level of Rp0.2 of the Al-Si alloy as well as optimizing their contents in order to obtain the highest values of the Al-Si alloy's proof stress Rp0.2. The analyses showed that each considered high-melting addition introduced into the Al-Si alloy in a proper amount can cause an increase of the proof stress Rp0.2 of the alloy, and the optimal content of each examined high-melting addition in respect of the highest obtained value of Rp0.2 equals 0.05%.
The work presents the results of the examinations of silumin 226 as well as a silumin produced on its basis containing a W and Mo addition introduced in the amount of 0.1; 0.2; 0.3 and 0.4% of both elements simultaneously. Investigations of the crystallization process of the silumins by the TDA method were conducted. Also, a microscopic analysis of their microstructure was performed and their basic mechanical properties were determined. Microstructure tests were made on casts produced in an TDA sampler as well as by the pressure method. The investigations exhibited a change in the course of crystallization of the silumin containing 0.3 and 0.4% W and Mo with respect to silumin 226 and the silumin with the addition of 0.1 and 0.2%. The presence of additional phases which did not occur in the case of lower addition contents was established in the silumin containing 0.3-0.4% W and Mo, regardless of the applied casting technology. The tests showed the possibility of increasing the tensile strength Rm, the proof stress Rp0,2 and the unit elongation A of the silumin as a result of a simultaneous introduction of the W and Mo addition. The highest values of Rm, Rp0,2 and A were obtained in the silumins with the additions of these elements within the range of 0.1-0.2% each.
Oxygen is used for medical treatment and general anesthesia. However, high concentrations of oxygen can have toxic effects on cells. In veterinary medicine, 100% oxygen is usually used during general anesthesia and it can be toxic to animals. However, there is little concern about its harmful effects in humans. The objective of this study was to demonstrate that using a high con- centration of oxygen increases the partial pressure of oxygen in arterial blood (PaO2) more so than a lower concentration, by comparing PaO2 at three different oxygen concentrations (100%, 60%, and 40%) in six dogs under general anesthesia for 3 hours. The mean PaO2 and standard error values at the 100%, 60%, and 40% oxygen concentrations were 535.8 ± 24.01, 374 ± 17.19, and 239 ± 8.78 mmHg, respectively (p<0.05). These results show that 100% and 60% oxygen concentrations could increase oxidative stress. Further studies are needed to examine the oxygen concentration that causes toxicity.
Gas-liquid flows abound in a great variety of industrial processes. Correct recognition of the regimes of a gasliquid flow is one of the most formidable challenges in multiphase flow measurement. Here we put forward a novel approach to the classification of gas-liquid flow patterns. In this method a flow-pattern map is constructed based on the average energy of intrinsic mode function and the volumetric void fraction of gas-liquid mixture. The intrinsic mode function is extracted from the pressure fluctuation across a bluff body using the empirical mode decomposition technique. Experiments adopting air and water as the working fluids are conducted in the bubble, plug, slug, and annular flow patterns at ambient temperature and atmospheric pressure. Verification tests indicate that the identification rate of the flow-pattern map developed exceeds 90%. This approach is appropriate for the gas-liquid flow pattern identification in practical applications.
To find effective and practical methods to distinguish gas-liquid two-phase flow patterns, new flow pattern maps are established using the differential pressure through a classical Venturi tube. The differential pressure signal was first decomposed adaptively into a series of intrinsic mode functions (IMFs) by the ensemble empirical mode decomposition. Hilbert marginal spectra of the IMFs showed that the flow patterns are related to the amplitude of the pressure fluctuation. The cross-correlation method was employed to sift the characteristic IMF, and then the energy ratio of the characteristic IMF to the raw signal was proposed to construct flow pattern maps with the volumetric void fraction and with the two-phase Reynolds number, respectively. The identification rates of these two maps are verified to be 91.18% and 92.65%. This approach provides a cost-effective solution to the difficult problem of identifying gas-liquid flow patterns in the industrial field.
The paper deals with problem of optimal used automatic workplace for HPDC technology - mainly from aspects of operations sequence, efficiency of work cycle and planning of using and servicing of HPDC casting machine. Presented are possible ways to analyse automatic units for HPDC. The experimental part was focused on the rationalization of the current work cycle time for die casting of aluminium alloy. The working place was described in detail in the project. The measurements were carried out in detail with the help of charts and graphs mapped cycle of casting workplace. Other parameters and settings have been identified. The proposals for improvements were made after the first measurements and these improvements were subsequently verified. The main actions were mainly software modifications of casting center. It is for the reason that today's sophisticated workplaces have the option of a relatively wide range of modifications without any physical harm to machines themselves. It is possible to change settings or unlock some unsatisfactory parameters.
The paper concerns the problem of discontinuity in high pressure die castings (HPDC). The compactness of their structure is not perfect, as it is sometimes believed. The discontinuities present in these castings are the porosity as follow: shrinkage and gas (hydrogen and gas-air occlusions) origin. The mixed gas and shrinkage nature of porosity makes it difficult to identify and indicate the dominant source. The selected parameters of metallurgical quality of AlSi9Cu3 alloy before and after refining and the gravity castings samples (as DI - density index method), were tested and evaluated. This alloy was served to cast the test casting by HPDC method. The penetrating testing (PT) and metallographic study of both kinds of castings were realized. The application of the NF&S simulation system allowed virtually to indicate the porosity zones at risk of a particular type in gravity and high-pressure-die-castings. The comparing of these results with the experiment allowed to conclude about NF&S models validation. The validity of hypotheses concerning the mechanisms of formation and development of porosity in HPDC casting were also analyzed.
A measuring system was developed for the measurement of ejector forces in the die casting process. When selecting the sensor technology, particular care was taken to ensure that measurements can be taken with a high sampling rate so that the fast-running ejection process can be recorded. For this reason, the system uses piezoelectric force sensors which measure the forces directly at the individual ejector pins. In this way, depending on the number of sensors, it is possible to determine both the individual ejector forces and the total ejector force. The system is expandable and adaptable with regard to the number and position of the sensors and can also be applied to real HPDC components. Automatic triggering of the measurements is also possible. In addition to the measuring system, a device and a method for in-situ calibration of the sensors have also been developed. To test the measuring system, casting experiments were carried out with a real aluminium HPDC aluminium component. The experiments showed that it is possible to measure the ejector forces with sufficient sampling rate and also to observe the process steps of filling, intensification and die opening by means of ejector forces. Experimental setup serves as a basis for future investigations regarding the influencing parameters on the ejection process.
The paper presents the mathematical modelling of selected isothermal separation processes of gaseous mixtures, taking place in plants using membranes, in particular nonporous polymer membranes. The modelling concerns membrane modules consisting of two channels - the feeding and the permeate channels. Different shapes of the channels cross-section were taken into account. Consideration was given to co-current and counter-current flows, for feeding and permeate streams, respectively, flowing together with the inert gas receiving permeate. In the proposed mathematical model it was considered that pressure of gas changes along the length of flow channels was the result of both - the drop of pressure connected with flow resistance, and energy transfer by molecules of gas flowing in a given channel to molecules which penetrate this channel from the adjacent channel. The literature on membrane technology takes into account only the drop of pressure connected with flow resistance. Consideration given to energy transfer by molecules of gas flowing in a given channel to molecules which penetrate this channel from the adjacent channel constitute the essential novelty in the current study. The paper also presents results of calculations obtained by means of a computer program which used equations of the derived model. Physicochemical data concerning separation of the CO2/CH4 mixture with He as the sweep gas and data concerning properties of the membrane made of PDMS were assumed for calculations.
The impact of casting conditions on microstructure a and mechanical properties was described, especially for cast products from AlSi9Cu3 alloy. Particular attention was paid to the parameters of dendritic structure: DAS 1 and DAS 2. Selected mechanical properties (by static tension test) of test castings made using basic technologies of casting: GSC - gravity sand casting, GDC - gravity die-casting and HPDC - high-pressure die-casting, are presented for cast-on test bars and cast separately. Casts were made of the same alloy AlSi9Cu3. Fractures and the zone near the fracture (after static tension test) was subjected to VT - visual tests, PT - penetration tests and metallographic tests. The condition of porosity (fracture zone) was also assessed. The analysis of virtual results was performed using the NovaFlow & Solid system together with the database and they were compared to experimental tests. This way of validation was applied in order to assess the correlation between the local rate of cooling and the size of DAS for GSC, GDC and HPDC technologies. Finally, the correlation between the parameters of structure and mechanical properties with regard to the impact of porosity was signalized.