Sound absorption coefficient is a commonly used parameter to characterize the acoustic properties of sound absorbing materials. It is defined within the frequency range of 100-5 000 Hz. In the industrial conditions, many appliances radiating acoustic energy of the frequency range of above 5000 Hz are used and at the same time it is known that a noise within the frequency range of 5 000-50 000 Hz can have a harmful effect on people,hence there is a need to define the coefficient in this frequency range. The article presents a proposal for a method of measurement of the sound absorption coefficient of materials in the frequency range from 5 000 Hz to 50 000 Hz. This method is a modification of the reverberation method with the use of interrupted noise.